MS Report from Instrument: LCMS-03 File ..ata\\20171108\\20171108-1\\BIZ2017-N08-WYQ14.D Tgt Mass (CHM): Injection Date : 8 Nov 17 2:40 pm +0800 Seq. Line : 22 Sample Name : BIZ2017-N08-WYQ14 Location : P1-E-09 Acq. Operator : SYSTEM Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\LCMS03\\Data\\20171108\\20171108-1\\1-POS-3MIN.M Analysis Method : D:\\LCMS03\\Data\\20171108\\20171108-1\\1-POS-3MIN.M Catalog No : HY-103663 Batch#27188 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 A, Sig=214,4 Ref=off1.3111.3401.374mAU500000.5 DAD1 B, Sig=254,4 Ref=offmAU200000.5 ELS1 A, ELSD SignalmV1005000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70300000020000001000000000.511.5 Ion 504.9, MSD1 504.9,Target Mass 503.9 +H Positive, EIC=504.6:505.6750050002500000.511.522.5min Integration Results for DAD1 A, Sig=214,4 Ref=off22.5min1.3701.522.5min11.40711.3111.3401.37311..4489391.5371.8162.2881.522.5min1.4441.4991.5371.8162.3021.522.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.31 0.01 2.97 4.44 0.32 377 1.34 0.02 909.80 1004.15 98.05 377 1.37 0.01 8.07 13.14 0.87 377 1.48 0.01 0.31 0.47 0.03 367 1.50 0.01 0.35 0.44 0.04 367 1.54 0.02 2.93 3.01 0.32 367 1.82 0.01 1.09 1.11 0.12 367 2.29 0.02 2.37 0.58 0.26 367 Integration Results for DAD1 B, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.31 0.01 1.35 2.04 0.28 377 1.34 0.02 473.90 521.28 98.03 377 1.37 0.01 4.59 7.15 0.95 377 1.44 0.01 0.15 0.18 0.03 377 1.50 0.02 0.22 0.15 0.05 367 1.54 0.02 1.53 1.42 0.32 367LCMS-03 11/9/2017 12:44:10 SYSTEMPage1 of4MS Report from Instrument: LCMS-03 1.82 0.02 0.36 0.29 0.07 367 2.30 0.02 1.32 1.08 0.27 367 Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.37 0.06 12017797.00 3241792.75 100.00 377LCMS-03 11/9/2017 12:44:10 SYSTEMPage2 of4MS Report from Instrument: LCMS-03Ret. Time: 1.37 <<<< POSITIVE SPECTRA >>>> ES-API Positive377.05000004000003000000100200300400500600700800900m/z189.2100000367.1378.0200000LCMS-03 11/9/2017 12:44:10 SYSTEMPage3 of4MS Report from Instrument: LCMS-03 *** End of Report ***LCMS-03 11/9/2017 12:44:10 SYSTEMPage4 of4